DSC 3500 Differential Scanning Calorimeter
DSC 3500 Differential Scanning Calorimeter
DSC 3500 Differential Scanning Calorimeter
DSC 3500 Differential Scanning Calorimeter
DSC 3500 Differential Scanning Calorimeter
DSC 3500 Differential Scanning Calorimeter
- Description:
DSC 3500 Differential Scanning Calorimeter
- Model:
DSC 3500
- Manufacturer:
NETZSCH
Product Information
  • Description
  • Standard
  • Feature
  • Specification
  • Configuration
  • Accessories
Description

差示扫描量热仪

Differential Scanning Calorimetry (DSC) is one of the frequently employed thermal analysis methods. It can be used to analyze nearly any energetic effect occurring in a solid or liquid during thermal treatment.


Easy handling and rapid analysis are among the hallmarks of this analytical technique, which has proven to be highly significant in the areas of research, development, and quality control. There are a variety of standards (ASTM, DIN,ISO, etc.) for the application, evaluation and interpretation of specific materials, products and properties.


The DSC 3500 Sirius operates according to the heat-flux principle. With this method, a sample and are ference are subjected to acontrolled temperature program(heating, cooling or isothermal).The actual measured properties are the temperature of the sample and the temperature difference between sample and reference. From the raw data signals, the heat flow difference between sample and reference can be determined which represents the caloric changes of the sample.


The gas-tight DSC 3500 Sirius combines the advantages of modern technology, high sensitivity and a robust, easy-to operate workhorse. Tests can be carried out in the temperature range between-170°C and 600°C.

Key components of the DSC 3500 Sirius are the DSC heat-flux sensor, the furnace and clever connection fittings which are designed for the quick and easy attachment of various cooling systems.

The sensor of the DSC 3500 Sirius combines high stability and optimized resolution of thermal effects. Laserguided welding processes for the sensor disks and thermocouple wires yield true sensitivity and robustness.


DSC features:

• Determination of onset, peak, inflection and end temperatures

• Automatic peak search

• Transformation enthalpies: analysis of peak areas (enthalpies) with selectable baseline and partial peak area analysis

• Evaluation of Crystallization

• Comprehensive Glass Transition analysis

• Automatic baseline correction

• Specific heat determination

• Tau-R® Mode: takes into account the time constant and thermal resistance of the instrument and reveals thus sharper DSC effects from the sample (optional)

• Optional TM-DSC (temperature modulation) for separation of reversing (thermodynamic) and non-reversing (kinetic) effects

Standard

• ISO 11357

• ASTM E793

• ASTM D3895

• ASTM D3418

• DIN 51004

• DIN 51007

• DIN 53765

Feature

• Reliable

Furnace and Sensor:Optimized design of the furnace and the sensor results in a highly stable baseline and excellent signal-to noise ratio.



• Variable

Gases and Cooling Options:Protective and purge gas inlets are, of course, standard features of the unit. For improved cooling times and subambient temperature tests, various cooling options can be connected. Of course, a versatile gas switching and flow control system are also available.



• Efficient

Automatic Sample Changer:For applications with a high sample throughput, we offer an automatic sample changer (ASC) for to 20samples and references which accommodates different crucible types. Flexibility and high sample throughput allow for efficient time management.



• All-Encompassing

Smart Instrumentation:Ease of handling is provided during measurement setup and evaluation by the SmartMode. This incorporates predefined measurement methods and wizards, Auto-Evaluation and Identify

Specification
DescriptionTechnical Specification
Temperature range-170℃~ 600℃
Heating/cooling rates0.001 K/min to 100 K/min (cooling rate depends on temperature)
Measurement range± 650 mW
AccuracyTemperature0.1 K  Enthalpy: < 1% for metals; < 2% for most materials
AtmospheresOxidizing, inert (static, dynamic)
Oxidative-InductionTimeIntegrated in the software
Dimensions380(560mm with ASC) x 320 x 520mm (H x W x D)
Weight28kg


Configuration
Accessories/Spare Parts

Accessories

• Variety of crucibles (Al, Pt, Al2O3, Au, Ag, Cu, autoclaves, etc.)

• For easy sample preparation, Sample Cutter and sample preparation kit


Cooling devices(options)

• Air compressor cooling: RT to 600°C

• Vortex cooling: 0°C to 600°C

• Intracooler IC 40: -40°C to 600°C; Intracooler IC 70: -70°C to 600°C

• Liquid nitrogen cooling: -170°C to 600°C

• Al cooling body


Software add-ons(optional)

• Temperature-modulated DSC

• Specific heat capacity (cp) determination

• Peak Separation

• Kinetics Neo

• AutoEvaluation

• Identify